Data base - II phase

location - Physical and chemical parameters

location - Chemical Analysis

Location 1

GPS coordinates: N 45°27’58.4″ E 019°54΄33.4″

Physical and Chemical parameters

Physical and chemical parameters at the Jegrička watercourse

Parameter	Value
T (°C)	29.8
O₂ (mg 1^-1)	5.75
O₂(%)	78.8
pH	7.56
CON (µS m^-1)	735
TSS (mg 1^-1)	24.8
TOC (mg 1^-1)	4.7
NO_3- (mg 1^-1)	<0.5
SUR (mg 1^-1)	1.2
COD (mg 1^-1)	13.6
BOD (mg 1^-1)	6.7
Transparency (cm)	35
Turbidity (cm)	48

Macrozoobenthos

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

Groups	Value
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus
Limnodrilus udekemianus
Limnodrilus sp.
Tubifex tubifex	39
Fam: Naididae
Dero sp.
Isopoda
Hydrachnidia
Ephemeroptera
Odonata
Diptera
Fam.Ceratopogonidae	78
Fam. Chironomidae	547
Total number	664

Microbiology

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality	Total number of heterotrophi c bacteria(CFU/ml)	Water class (kohl, 1975)	Number of facultative oligotrophic bacteria (CFU/ml)	Index FO/H	Autopurification ability	Total number of Coliform bacteria(CFU/ml)	Number of fecal Coliform bacteria(CFU/ml)	Water class (Kavka, 1994)
1	850	I-II	600	0.71	week	65	0	mildly polluted

Location 2

GPS coordinates: N 45°27’23.1″ E 019°53΄0.95″

Physical and Chemical parameters

Physical and chemical parameters at the Jegrička watercourse

Parameter	Value
T (°C)	28.9
O₂ (mg 1^-1)	3.05
O₂(%)	37
pH	7.34
CON (µS m^-1)	675
TSS (mg 1^-1)	23.6
TOC (mg 1^-1)	4.1
NO_3- (mg 1^-1)	<0.5
SUR (mg 1^-1)	0.9
COD (mg 1^-1)	12.1
BOD (mg 1^-1)	5.8
Transparency (cm)	30
Turbidity (cm)	32

Macrozoobenthos

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

Groups	Value
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri	78
Limnodrilus claparedeanus
Limnodrilus udekemianus
Limnodrilus sp.
Tubifex tubifex
Fam: Naididae
Dero sp.
Isopoda
Hydrachnidia
Ephemeroptera
Odonata
Diptera
Fam.Ceratopogonidae	39
Fam. Chironomidae	235
Total number	352

Microbiology

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality	Total number of heterotrophi c bacteria(CFU/ml)	Water class (kohl, 1975)	Number of facultative oligotrophic bacteria (CFU/ml)	Index FO/H	Autopurification ability	Total number of Coliform bacteria(CFU/ml)	Number of fecal Coliform bacteria(CFU/ml)	Water class (Kavka, 1994)
2	1500	II	2650	1.77	satisfactory	370	50	mildly polluted

Location 3

GPS coordinates: N 45°27’18.1″ E 019°48΄38.9″

Physical and Chemical parameters

Physical and chemical parameters at the Jegrička watercourse

Parameter	Value
T (°C)	26.9
O₂ (mg 1^-1)	1.1
O₂(%)	14
pH	7.14
CON (µS m^-1)	596
TSS (mg 1^-1)	12.5
TOC (mg 1^-1)	3.7
NO_3- (mg 1^-1)	<0.5
SUR (mg 1^-1)	0.8
COD (mg 1^-1)	10.8
BOD (mg 1^-1)	5.3
Transparency (cm)	45
Turbidity (cm)	50

Macrozoobenthos

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

Groups	Value
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus	39
Limnodrilus udekemianus
Limnodrilus sp.	39
Tubifex tubifex	39
Fam: Naididae
Dero sp.
Isopoda
Hydrachnidia
Ephemeroptera
Odonata
Diptera
Fam.Ceratopogonidae	508
Fam. Chironomidae	196
Total number	821

Microbiology

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality	Total number of heterotrophi c bacteria(CFU/ml)	Water class (kohl, 1975)	Number of facultative oligotrophic bacteria (CFU/ml)	Index FO/H	Autopurification ability	Total number of Coliform bacteria(CFU/ml)	Number of fecal Coliform bacteria(CFU/ml)	Water class (Kavka, 1994)
3	1000	II	2300	2.3	satisfactory	140	20	polluted

Location 4

GPS coordinates: N 45°27’16.0″ E 019°43΄48.1″

Physical and Chemical parameters

Physical and chemical parameters at the Jegrička watercourse

Parameter	Value
T (°C)	26.9
O₂ (mg 1^-1)	16.18
O₂(%)	210
pH	8.24
CON (µS m^-1)	1086
TSS (mg 1^-1)	26.6
TOC (mg 1^-1)	5.3
NO_3- (mg 1^-1)	<0.5
SUR (mg 1^-1)	0.9
COD (mg 1^-1)	16
BOD (mg 1^-1)	1.6
Transparency (cm)	21
Turbidity (cm)	31

Macrozoobenthos

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

Groups	Value
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus	156
Limnodrilus udekemianus	39
Limnodrilus sp.	821
Tubifex tubifex	117
Fam: Naididae
Dero sp.	78
Isopoda
Hydrachnidia
Ephemeroptera
Odonata
Diptera
Fam.Ceratopogonidae	196
Fam. Chironomidae	430
Total number	1837

Microbiology

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality	Total number of heterotrophi c bacteria(CFU/ml)	Water class (kohl, 1975)	Number of facultative oligotrophic bacteria (CFU/ml)	Index FO/H	Autopurification ability	Total number of Coliform bacteria(CFU/ml)	Number of fecal Coliform bacteria(CFU/ml)	Water class (Kavka, 1994)
4	3500	II	4780	1.45	satisfactory	260	90	Very polluted

Location 5

GPS coordinates: N 45°27’03.0″ E 019°42΄32.9″

Physical and Chemical parameters

Physical and chemical parameters at the Jegrička watercourse

Parameter	Value
T (°C)	27.7
O₂ (mg 1^-1)	6.42
O₂(%)	83.4
pH	7.66
CON (µS m^-1)	961
TSS (mg 1^-1)	26.4
TOC (mg 1^-1)	5.2
NO_3- (mg 1^-1)	<0.5
SUR (mg 1^-1)	0.9
COD (mg 1^-1)	15.6
BOD (mg 1^-1)	7.5
Transparency (cm)	50
Turbidity (cm)	56

Macrozoobenthos

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

Groups	Value
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri	235
Limnodrilus claparedeanus	196
Limnodrilus udekemianus
Limnodrilus sp.	430
Tubifex tubifex	313
Fam: Naididae
Dero sp.	78
Isopoda	39
Hydrachnidia	39
Ephemeroptera	352
Odonata	196
Diptera
Fam.Ceratopogonidae	117
Fam. Chironomidae	587
Total number	2582

Microbiology

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality	Total number of heterotrophi c bacteria(CFU/ml)	Water class (kohl, 1975)	Number of facultative oligotrophic bacteria (CFU/ml)	Index FO/H	Autopurification ability	Total number of Coliform bacteria(CFU/ml)	Number of fecal Coliform bacteria(CFU/ml)	Water class (Kavka, 1994)
5	3300	II	4780	1.45	satisfactory	260	90	Very polluted

Chemical Analysis - surface water

Type of sample:	surface water
Sampling location:	Jegricka, near Temerin
Coordinates of sampling location:	SRPS ISO 5667-6:2017, SRPS EN ISO 5667-1:2008
Sampling procedure:
Date and time of sampling:	27.06.2019.

Examined parameter	*Unit of measure*	Method designation	Measured value	Class**
Air temperature	^oC	SRPS H.Z1.106:1970	*20,2*	–
Water temperature	^oC	SRPS H.Z1.106:1970	*19,5*	–
Colour*	opisno	vizuelno	*bistra*	–
Smell*	opisno	vizuelno	*bez*	–
Visible substances*	opisno	vizuelno	*bez*	–
pH		SRPS H.Z1.111:1987	*7,71*	I
Electroconductivity	µS/cm	SRPS EN 27888:2009	*694*	I
Dissolved oxygen	mgO₂ /l	SRPS EN 5814:2014	*2,51*	V
Suspended substances	mg/l	SM 2540 D	*<12*	I
Total dry residue	mg/l	SM 2540 B	*414*	I
HPK	mgO₂/l	SRPS ISO 6060:1994	*<32*	II/III
BPK5	mg O₂/l	H1.002	29	V
Total nitrogen	mgN/l	H1.011	*0,621*	I
Total Kjeldahl nitrogen	mgN/l	H1.003	*0,591*	–
Ammonium ion	mgN/l	SRPS ISO H.Z1.184:1974	*<0,06*	I
Nitrates	mgN/l	SRPS ISO 7890-3:1994	*0,030*	I
Nitrites	mgN/l	SRPS EN 26777:2009	*<0,005*	I
Total phosphorus	mgP/l	SRPS EN ISO 6878:2008	*0,564*	I
Orthophosphates	mgP/l	SRPS EN ISO 6878:2008	*0,133*	I
Sulphides	mgS/l	SM 4500-S^2- E	*0,7*	–
Anionicdetergents	mg/l	SRPS EN 903:2009	*<0,12*	I/II
Carbon Dioxide index	mg/l	ISO 9377-2:2000(E)	*<2,02*	–
*Metals*
Iron	mg/l	EPA 7000b	*0,300*	II
Manganese	µg/l	EPA 7010	*73,7*	II
Nickel	µg/l	EPA 7010	*<2,2*	I
Zinc	mg/l	EPA 7000b	*<0,023*	I
Cadmium	µg/l	EPA 7010	*<0,15*	I
Chromium, total	µg/l	EPA 7010	*<0,90*	I
Copper	µg/l	EPA 7010	*<0,9*	I
Lead	µg/l	EPA 7010	*<5,9*	I
Mercury	µg/l	H1.004	*<0,5*	I
*VOC*
Hloroform	µg/l	H1.001	*<1,60*	–
1.1.1-trihloretan (1.1.1-TCE)	µg/l		*<0,260*	–
1.2-dihloretan (1.2-DCE)	µg/l		*<0,245*	–
Benzen	µg/l		*<0,365*	–
Trihloretilen	µg/l		*<0,605*	–
BDHM	µg/l		*<0,480*	–
Toluol	µg/l		*3,25*	–
DBHM	µg/l		*<0,480*	–
Tetrahloroetilen	µg/l		*<0,510*	–
Hlorbenzen	µg/l		*<0,620*	–
Etilbenzen	µg/l		*<0,650*	–
m+p-ksilen	µg/l		*<0,780*	–
o-ksilen	µg/l		*<1,03*	–
Bromoform	µg/l		*<0,720*	–
1,2-dihlorobenzen	µg/l		*<1,15*	–
1,4-dihlorobenzen	µg/l		*<1,32*	–
Vinilhlorid	µg/l		*<0,500*	–
Pesticidi				–
alfa-HCH	ng/l	SM 6630	*<5,00*	–
beta-HCH	ng/l		*<5,00*	–
gama-HCH (lindan)	ng/l		*<3,25*	–
delta-HCH	ng/l		*<2,50*	–
Heptahlor	ng/l		*<2,50*	–
Heptahlorepoksid	ng/l		*<2,50*	–
Aldrin	ng/l		*<2,50*	–
Dieldrin	ng/l		*<6,25*	–
Endrin	ng/l		*<6,25*	–
Endrinaldehid	ng/l		*<1,75*	–
Endosulfansulfat	ng/l		*<2,50*	–
Endosulfan I	ng/l		*<2,50*	–
Endosulfan II	ng/l		*<2,50*	–
4,4´-DDT	ng/l		*<0,500*	–
4,4´-DDD	ng/l		*<2,00*	–
4,4´-DDE	ng/l		*<4,75*	–
PAH				–
Naftalen	ng/l	SM 6440	*14,4*	–
Acenaftilen	ng/l		*<9,00*	–
Acenaften	ng/l		*<10,3*	–
Fluoren	ng/l		*21,6*	–
Fenantren	ng/l		*7,92*	–
Antracen	ng/l		*7,8*	–
Fluoranten	ng/l		*<6,50*	–
Piren	ng/l		*<4,45*	–
Benzo(a)antracen	ng/l		*<19,1*	–
Krizen	ng/l		*<20,5*	–
Benzo(b)fluoranten+ Benzo(k)fluoranten	ng/l		*49,6*	–
Benzo(a)piren	ng/l		*<30,0*	–
Benzo(g,h,i)perilen	ng/l		*<30,0*	–
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren	ng/l		*<30,0*	–

*Parameter/method not within accreditation

**According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Chemical Analysis - surface water

Type of sample:	surface water
Sampling location:	Jegrička - downstream of station Zmajevo
Coordinates of sampling location:
Sampling procedure:	SRPS ISO 5667-6:2017, SRPS EN ISO 5667-1:2008
Date and time of sampling:	05.07.2019.

Examined parameter	*Unit of measure*	Method designation	Measured value	Class**
Air temperature	^oC	SRPS H.Z1.106:1970	*28,5*	–
Water temperature	^oC	SRPS H.Z1.106:1970	*25,5*	–
Colour*	opisno	vizuelno	*bistra*	–
Smell*	opisno	vizuelno	*bez*	–
Visible substances*	opisno	vizuelno	*bez*	–
pH		SRPS H.Z1.111:1987	*7,61*	I
Electroconductivity	µS/cm	SRPS EN 27888:2009	*525*	I
Dissolved oxygen	mgO₂ /l	SRPS EN 5814:2014	*2,52*	V
Suspended substances	mg/l	SM 2540 D	*<12*	I
Total dry residue	mg/l	SM 2540 B	*319*	I
HPK	mgO₂/l	SRPS ISO 6060:1994	*<32*	II/III
BPK5	mg O₂/l	H1.002	25	V
Total nitrogen	mgN/l	H1.011	*0,686*	I
Total Kjeldahl nitrogen	mgN/l	H1.003	*0,591*	–
Ammonium ion	mgN/l	SRPS ISO H.Z1.184:1974	*<0,06*	I
Nitrates	mgN/l	SRPS ISO 7890-3:1994	*0,095*	I
Nitrites	mgN/l	SRPS EN 26777:2009	*<0,005*	I
Total phosphorus	mgP/l	SRPS EN ISO 6878:2008	*0,096*	I
Orthophosphates	mgP/l	SRPS EN ISO 6878:2008	*0,082*	I
Sulphides	mgS/l	SM 4500-S^2- E	*<0,50*	–
Anionicdetergents	mg/l	SRPS EN 903:2009	*<0,12*	I/II
Carbon Dioxide index	mg/l	ISO 9377-2:2000(E)	*<2,02*	–
*Metals*
Iron	mg/l	EPA 7000b	*0,458*	II
Manganese	µg/l	EPA 7010	*34,5*	I
Nickel	µg/l	EPA 7010	*4,89*	II
Zinc	mg/l	EPA 7000b	*<0,023*	I
Cadmium	µg/l	EPA 7010	*<0,15*	I
Chromium, total	µg/l	EPA 7010	*<0,90*	I
Copper	µg/l	EPA 7010	*2,59*	I
Lead	µg/l	EPA 7010	*<5,9*	I
Mercury	µg/l	H1.004	*<0,5*	I
*VOC*
Chloroform	µg/l	H1.001	*7,00*	–
1.1.1-trichloroethane (1.1.1-TCE)	µg/l		*<0,260*	–
1.2-dichloroethane (1.2-DCE)	µg/l		*<0,245*	–
Benzene	µg/l		*<0,365*	–
Trichlorethylene	µg/l		*<0,605*	–
BDHM	µg/l		*<0,480*	–
Toluene	µg/l		*<1,06*	–
DBHM	µg/l		*<0,480*	–
Tetrachloroethylene	µg/l		*<0,510*	–
Chlorobenzene	µg/l		*<0,620*	–
Ethylbenzene	µg/l		*<0,650*	–
m+p-xylene	µg/l		*<0,780*	–
o-xylene	µg/l		*1,15*	–
Bromoform	µg/l		*<0,720*	–
1,2-dichlorobenzene	µg/l		*<1,15*	–
1,4-dichlorobenzene	µg/l		*<1,32*	–
VinylChloride	µg/l		*<0,500*	–
Pesticidi				–
alpha-HCH	ng/l	SM 6630	*<5,00*	–
beta-HCH	ng/l		*15,5*	–
gama-HCH (lindan)	ng/l		*<3,25*	–
delta-HCH	ng/l		*<2,50*	–
Heptachlor	ng/l		*<2,50*	–
Heptachlor Epoxide	ng/l		*<2,50*	–
Aldrin	ng/l		*<2,50*	–
Dieldrin	ng/l		*<6,25*	–
Endrin	ng/l		*<6,25*	–
Endrin Aldehyde	ng/l		*<1,75*	–
Endosulfan Sulfate	ng/l		*<2,50*	–
Endosulfan I	ng/l		*<2,50*	–
Endosulfan II	ng/l		*<2,50*	–
4,4´-DDT	ng/l		*<0,500*	–
4,4´-DDD	ng/l		*<2,00*	–
4,4´-DDE	ng/l		*<4,75*	–
PAH				–
Naftalen	ng/l	SM 6440	*48,7*	–
Acenaphthylene	ng/l		*<9,00*	–
Acenaphthene	ng/l		*<10,3*	–
Fluorene	ng/l		*15,6*	–
Phenanthrene	ng/l		*18,2*	–
Anthracene	ng/l		*34,4*	–
Fluoranten	ng/l		*<6,50*	–
Pyrene	ng/l		*<4,45*	–
Benzo(a)anthracene	ng/l		*<19,1*	–
Chrysene	ng/l		*<20,5*	–
Benzo(b)fluoranthene + Benzo(k)fluoranthene	ng/l		*54,5*	–
Benzo(a)pyrene	ng/l		*<30,0*	–
Benzo(g,h,i)perylene	ng/l		*<30,0*	–
Dibenzo(a,h)anthracene + Indeno(1,2,3-cd)pyrene	ng/l		*<30,0*	–

*Parameter/method not within accreditation

**According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Chemical Analysis - sediment

Type of sample:	sediment
Sampling location:	Jegrička – near Temerin
Coordinates of sampling location:
Sampling procedure:
Date and time of sampling:	27.06.2019.

Examined parameter	*Unit of measure*	Method designation	Measured value	Adjusted value	Class**
vlaga	%	SRPS EN 12880:2007	*15,0*	–	–
gubitak žarenjem	%	SRPS EN 12879:2007	*5,90*	–	–
granulometrija (čestice <2µm)	%	ISO 11277:2009	*24,6*	–	–
pH		SRPS EN 12176:2005	*8,38*
Redoks potencijal
Ukupan azot	mgN/kg	SRPS ISO 11261:2005	*1133*	–	–
organski + amonijačni azot*	mgN/kg	destilacija i titracija	*826*	–	–
nitratni + nitritni azot*	mgN/kg	destilacija i titracija	*307*	–	–
Ukupan fosfor*	mgP/kg	spektrofotometrija	*266*	–	–
*Metali*
Nikl	mg/kg	EPA 7010	*28,8*	29,1	0
Cink	mg/kg	EPA 7000b	*58,8*	62,0	0
Kadmijum	mg/kg	EPA 7010	*0,14*	0,16	0
Hrom, ukupan	mg/kg	EPA 7010	*18,1*	18,3	0
Bakar	mg/kg	EPA 7010	*20,4*	22,1	0
Olovo	mg/kg	EPA 7010	*8,82*	9,31	0
Arsen	mg/kg	EPA 7010	*7,00*	7,46	0
Živa	mg/kg	H1.005	*0,071*	0,07	0
Pesticidi
alfa-HCH	µg/kg	H1.008 (GC/µECD)	*<10,1*	–	–
beta-HCH	µg/kg		*<10,5*	–	–
gama-HCH (lindan)	µg/kg		*<7,68*	–	–
delta-HCH	µg/kg		*<6,53*	–	–
Heptahlor	µg/kg		*<6,53*	–	–
Heptahlorepoksid	µg/kg		*<9,22*	–	–
Aldrin	µg/kg		*<8,39*	–	–
Dieldrin	µg/kg		*<7,92*	–	–
Endrin	µg/kg		*<7,24*	–	–
Endrinaldehid	µg/kg		*<10,4*	–	–
Endosulfansulfat	µg/kg		*<9,88*	–	–
Endosulfan I	µg/kg		*<5,26*	–	–
Endosulfan II	µg/kg		*<9,10*	–	–
4,4´-DDT	µg/kg		*<0,500*	–	–
4,4´-DDD	µg/kg		*<3,77*	–	–
4,4´-DDE	µg/kg		*<9,58*	–	–
Prioritetni pesticidi*
Pentahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
Heksahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
PAH	µg/kg		*15,4*	15,4	0
Naftalen	µg/kg	H1.009 (GC/MSD)	*15,4*	–	–
Acenaftilen	µg/kg		*<6,69*	–	–
Acenaften	µg/kg		*<3,88*	–	–
Fluoren	µg/kg		*<10,6*	–	–
Fenantren	µg/kg		*<9,26*	–	–
Antracen	µg/kg		*<10,8*	–	–
Fluoranten	µg/kg		*<9,80*	–	–
Piren	µg/kg		*<9,92*	–	–
Benzo(a)antracen	µg/kg		*<11,1*	–	–
Krizen	µg/kg		*<9,88*	–	–
Benzo(b)fluoranten+ Benzo(k)fluoranten	µg/kg		*<9,23*	–	–
Benzo(a)piren	µg/kg		*<11,1*	–	–
Benzo(g,h,i)perilen	µg/kg		*<11,9*	–	–
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren	µg/kg		*<10,5*	–	–
PCB (suma)	µg/kg	H1.008 (GC/µECD)	*<9,63*	–	0
Dihlorbifenil (PCB 10)	µg/kg		*<9,63*	–	–
2,4,4´-trihlorbifenil (PCB 28)	µg/kg		*<5,26*	–	–
2,2´,5,5´- tetrahlorbifenil (PCB 52)	µg/kg		*<7,74*	–	–
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138)	µg/kg		*<2,81*	–	–
2,2′,4,4′,5,5′-heksahlorbifenil (PCB 153)	µg/kg		*<7,30*	–	–
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180)	µg/kg		*<2,08*	–	–
Indeks ugljovodonika*	mg/kg		*72,9*	124	1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Chemical Analysis - sediment

Type of sample:	sediment
Sampling location:	Jegricka, near Temerin
Coordinates of sampling location:
Sampling procedure:	SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling:	27.06.2019.

Examined parameter	*Unit of measure*	Method designation	Measured value	Corrected value	Classifiation**
vlaga	%	SRPS EN 12880:2007	*19,2*	–	–
gubitak žarenjem	%	SRPS EN 12879:2007	*8,38*	–	–
granulometrija (čestice <2µm)	%	ISO 11277:2009	*30,4*	–	–
pH		SRPS EN 12176:2005	*8,25*
Redoks potencijal
Ukupan azot	mgN/kg	SRPS ISO 11261:2005	*1237*	–	–
organski + amonijačni azot*	mgN/kg	destilacija i titracija	*968*	–	–
nitratni + nitritni azot*	mgN/kg	destilacija i titracija	*269*	–	–
Ukupan fosfor*	mgP/kg	spektrofotometrija	*306*	–	–
*Metali*
Nikl	mg/kg	EPA 7010	*32,8*	28,4	0
Cink	mg/kg	EPA 7000b	*75,2*	68,5	0
Kadmijum	mg/kg	EPA 7010	*0,23*	0,23	0
Hrom, ukupan	mg/kg	EPA 7010	*35,3*	31,9	0
Bakar	mg/kg	EPA 7010	*27,9*	26,2	0
Olovo	mg/kg	EPA 7010	*13,5*	12,9	0
Arsen	mg/kg	EPA 7010	*16,5*	15,7	0
Živa	mg/kg	H1.005	*0,068*	0,07	0
Pesticidi
alfa-HCH	µg/kg	H1.008 (GC/µECD)	*<10,1*	–	–
beta-HCH	µg/kg		*<10,5*	–	–
gama-HCH (lindan)	µg/kg		*<7,68*	–	–
delta-HCH	µg/kg		*<6,53*	–	–
Heptahlor	µg/kg		*<6,53*	–	–
Heptahlorepoksid	µg/kg		*<9,22*	–	–
Aldrin	µg/kg		*<8,39*	–	–
Dieldrin	µg/kg		*<7,92*	–	–
Endrin	µg/kg		*<7,24*	–	–
Endrinaldehid	µg/kg		*<10,4*	–	–
Endosulfansulfat	µg/kg		*<9,88*	–	–
Endosulfan I	µg/kg		*<5,26*	–	–
Endosulfan II	µg/kg		*<9,10*	–	–
4,4´-DDT	µg/kg		*<0,500*	–	–
4,4´-DDD	µg/kg		*<3,77*	–	–
4,4´-DDE	µg/kg		*<9,58*	–	–
Prioritetni pesticidi*
Pentahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
Heksahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
PAH	µg/kg		60	60	0
Naftalen	µg/kg	H1.009 (GC/MSD)	*8,94*	–	–
Acenaftilen	µg/kg		*<6,69*	–	–
Acenaften	µg/kg		*<3,88*	–	–
Fluoren	µg/kg		*<10,6*	–	–
Fenantren	µg/kg		*<9,26*	–	–
Antracen	µg/kg		*<10,8*	–	–
Fluoranten	µg/kg		*<9,80*	–	–
Piren	µg/kg		*<9,92*	–	–
Benzo(a)antracen	µg/kg		*<11,1*	–	–
Krizen	µg/kg		*<9,88*	–	–
Benzo(b)fluoranten+ Benzo(k)fluoranten	µg/kg		*<9,23*	–	–
Benzo(a)piren	µg/kg		*<11,1*	–	–
Benzo(g,h,i)perilen	µg/kg		*<11,9*	–	–
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren	µg/kg		*50,7*	–	–
PCB (suma)	µg/kg	H1.008 (GC/µECD)	*<9,63*	–	0
Dihlorbifenil (PCB 10)	µg/kg		*<9,63*	–	–
2,4,4´-trihlorbifenil (PCB 28)	µg/kg		*<5,26*	–	–
2,2´,5,5´- tetrahlorbifenil (PCB 52)	µg/kg		*<7,74*	–	–
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138)	µg/kg		*<2,81*	–	–
2,2′,4,4′,5,5′-heksahlorbifenil (PCB 153)	µg/kg		*<7,30*	–	–
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180)	µg/kg		*<2,08*	–	–
Indeks ugljovodonika*	mg/kg		*52,4*	62,5	1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Chemical Analysis - sediment

Type of sample:	sediment
Sampling location:	Jegricka, near Temerin
Coordinates of sampling location:
Sampling procedure:	SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling:	27.06.2019.

Examined parameter	*Unit of measure*	Method designation	Measured value	Adjusted valuet	Class**
vlaga	%	SRPS EN 12880:2007	*78,1*	–	–
gubitak žarenjem	%	SRPS EN 12879:2007	*18,5*	–	–
granulometrija (čestice <2µm)	%	ISO 11277:2009	*29,8*	–	–
pH		SRPS EN 12176:2005	*7,85*
Redoks potencijal
Ukupan azot	mgN/kg	SRPS ISO 11261:2005	*1132*	–	–
organski + amonijačni azot*	mgN/kg	destilacija i titracija	*888*	–	–
nitratni + nitritni azot*	mgN/kg	destilacija i titracija	*244*	–	–
Ukupan fosfor*	mgP/kg	spektrofotometrija	*255*	–	–
*Metali*
Nikl	mg/kg	EPA 7010	*27,7*	24,3	0
Cink	mg/kg	EPA 7000b	*74,2*	62,1	0
Kadmijum	mg/kg	EPA 7010	*0,29*	0,22	0
Hrom, ukupan	mg/kg	EPA 7010	*28,4*	25,9	0
Bakar	mg/kg	EPA 7010	*27,6*	22,6	0
Olovo	mg/kg	EPA 7010	*17,5*	15,1	0
Arsen	mg/kg	EPA 7010	*41,0*	34,6	1
Živa	mg/kg	H1.005	*0,126*	0,11	0
Pesticidi
alfa-HCH	µg/kg	H1.008 (GC/µECD)	*<10,1*	–	–
beta-HCH	µg/kg		*<10,5*	–	–
gama-HCH (lindan)	µg/kg		*<7,68*	–	–
delta-HCH	µg/kg		*<6,53*	–	–
Heptahlor	µg/kg		*<6,53*	–	–
Heptahlorepoksid	µg/kg		*<9,22*	–	–
Aldrin	µg/kg		*<8,39*	–	–
Dieldrin	µg/kg		*<7,92*	–	–
Endrin	µg/kg		*<7,24*	–	–
Endrinaldehid	µg/kg		*<10,4*	–	–
Endosulfansulfat	µg/kg		*<9,88*	–	–
Endosulfan I	µg/kg		*<5,26*	–	–
Endosulfan II	µg/kg		*<9,10*	–	–
4,4´-DDT	µg/kg		*2,48*	–	–
4,4´-DDD	µg/kg		*<3,77*	–	–
4,4´-DDE	µg/kg		*<9,58*	–	–
Prioritetni pesticidi*
Pentahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
Heksahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
PAH	µg/kg		*1655*	1655	2
Naftalen	µg/kg	H1.009 (GC/MSD)	*143*	–	–
Acenaftilen	µg/kg		*37,8*	–	–
Acenaften	µg/kg		*4,95*	–	–
Fluoren	µg/kg		*35,4*	–	–
Fenantren	µg/kg		*73,0*	–	–
Antracen	µg/kg		*41,3*	–	–
Fluoranten	µg/kg		*251*	–	–
Piren	µg/kg		*246*	–	–
Benzo(a)antracen	µg/kg		*12,8*	–	–
Krizen	µg/kg		*17,5*	–	–
Benzo(b)fluoranten+ Benzo(k)fluoranten	µg/kg		*454*	–	–
Benzo(a)piren	µg/kg		*69,2*	–	–
Benzo(g,h,i)perilen	µg/kg		*214*	–	–
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren	µg/kg		*379*	–	–
PCB (suma)	µg/kg	H1.008 (GC/µECD)	*<9,63*	–	0
Dihlorbifenil (PCB 10)	µg/kg		*<9,63*	–	–
2,4,4´-trihlorbifenil (PCB 28)	µg/kg		*<5,26*	–	–
2,2´,5,5´- tetrahlorbifenil (PCB 52)	µg/kg		*<7,74*	–	–
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138)	µg/kg		*<2,81*	–	–
2,2′,4,4′,5,5′-heksahlorbifenil (PCB 153)	µg/kg		*<7,30*	–	–
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180)	µg/kg		*<2,08*	–	–
Indeks ugljovodonika*	mg/kg		*390*	211	1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Chemical Analysis - sediment

Type of sample:	sediment
Sampling location:	Jegricka, near Zmajevo
Coordinates of sampling location:
Sampling procedure:	SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling:	05.07.2019.

Ispitivani parametar	*Jed. mere*	Oznaka metode	Izmerena vrednost	Korigovana vrednost	Klasifika-cija**
vlaga	%	SRPS EN 12880:2007	*13,9*	–	–
gubitak žarenjem	%	SRPS EN 12879:2007	*9,80*	–	–
granulometrija (čestice <2µm)	%	ISO 11277:2009	*43,7*	–	–
pH		SRPS EN 12176:2005	*8,47*
Redoks potencijal
Ukupan azot	mgN/kg	SRPS ISO 11261:2005	*1271*	–	–
organski + amonijačni azot*	mgN/kg	destilacija i titracija	*965*	–	–
nitratni + nitritni azot*	mgN/kg	destilacija i titracija	*306*	–	–
Ukupan fosfor*	mgP/kg	spektrofotometrija	*233*	–	–
*Metali*
Nikl	mg/kg	EPA 7010	*33,7*	20,9	0
Cink	mg/kg	EPA 7000b	*80,4*	55,2	0
Kadmijum	mg/kg	EPA 7010	*0,344*	0,29	0
Hrom, ukupan	mg/kg	EPA 7010	*25,0*	17,5	0
Bakar	mg/kg	EPA 7010	*37,9*	28,0	0
Olovo	mg/kg	EPA 7010	*18,1*	14,4	0
Arsen	mg/kg	EPA 7010	*29,2*	22,5	0
Živa	mg/kg	H1.005	*0,052*	0,04	0
Pesticidi
alfa-HCH	µg/kg	H1.008 (GC/µECD)	*<10,1*	–	–
beta-HCH	µg/kg		*<10,5*	–	–
gama-HCH (lindan)	µg/kg		*<7,68*	–	–
delta-HCH	µg/kg		*<6,53*	–	–
Heptahlor	µg/kg		*<6,53*	–	–
Heptahlorepoksid	µg/kg		*<9,22*	–	–
Aldrin	µg/kg		*<8,39*	–	–
Dieldrin	µg/kg		*<7,92*	–	–
Endrin	µg/kg		*<7,24*	–	–
Endrinaldehid	µg/kg		*<10,4*	–	–
Endosulfansulfat	µg/kg		*<9,88*	–	–
Endosulfan I	µg/kg		*<5,26*	–	–
Endosulfan II	µg/kg		*<9,10*	–	–
4,4´-DDT	µg/kg		*0,741*	–	–
4,4´-DDD	µg/kg		*<3,77*	–	–
4,4´-DDE	µg/kg		*<9,58*	–	–
Prioritetni pesticidi*
Pentahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
Heksahlorbenzen	µg/kg	H1.009 (GC/MSD)	*<0,500*	–	–
PAH	µg/kg		19	19	0
Naftalen	µg/kg	H1.009 (GC/MSD)	*9,46*	–	–
Acenaftilen	µg/kg		*<6,69*	–	–
Acenaften	µg/kg		*<3,88*	–	–
Fluoren	µg/kg		*<10,6*	–	–
Fenantren	µg/kg		*<9,26*	–	–
Antracen	µg/kg		*<10,8*	–	–
Fluoranten	µg/kg		*<9,80*	–	–
Piren	µg/kg		*<9,92*	–	–
Benzo(a)antracen	µg/kg		*<11,1*	–	–
Krizen	µg/kg		*<9,88*	–	–
Benzo(b)fluoranten+ Benzo(k)fluoranten	µg/kg		*9,46*	–	–
Benzo(a)piren	µg/kg		*<11,1*	–	–
Benzo(g,h,i)perilen	µg/kg		*<11,9*	–	–
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren	µg/kg		*<10,5*	–	–
PCB (suma)	µg/kg	H1.008 (GC/µECD)	*<9,63*	–	0
Dihlorbifenil (PCB 10)	µg/kg		*<9,63*	–	–
2,4,4´-trihlorbifenil (PCB 28)	µg/kg		*<5,26*	–	–
2,2´,5,5´- tetrahlorbifenil (PCB 52)	µg/kg		*<7,74*	–	–
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138)	µg/kg		*<2,81*	–	–
2,2′,4,4′,5,5′-heksahlorbifenil (PCB 153)	µg/kg		*<7,30*	–	–
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180)	µg/kg		*<2,08*	–	–
Indeks ugljovodonika*	mg/kg		*80,1*	81,7	1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)