Data base - I phase

location - Physical and chemical parameters

location - Chemical Analysis

Location 1

GPS coordinates: N 45°27’59.20″ E19°54’38.58″


Physical and chemical parameters at the Jegrička watercourse

ParameterValue
T (°C) 17.2
O2 (mg 1-1) 1.17
O2(%) 14.4
pH 7.6
CON (µS m-1) 926
TSS (mg 1-1) 13.8
TOC (mg 1-1) 6.2
NO3- (mg 1-1) <0.5
SUR (mg 1-1) 1.7
COD (mg 1-1) 17.6
BOD (mg 1-1) 9
Transparency (cm) 115
Turbidity (cm) 140

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

GroupsValue
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri 39
Limnodrilus claparedeanus
Limnodrilus sp. 78
Tubifex tubifex 1720
Potamotrix hammoniensis
Fam: Naididae
Nais elinguis
Nais variabilis
Stylaria lacustris 39
Ophidonais serpentina 626
Hirudinea
Helobdella stagnalis 39
Isopoda
Asellus aquaticus 430
Ephemeroptera
Fam: Caenidae
Caenis robusta 156
Odonata
Diptera
Fam: Ceratopogonidae
Bezzia sp. 39
Fam: Culicidae 78
Fam: Chironomidae 978
Total number 4222

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality Total number of heterotrophi c bacteria(CFU/ml) Water class (kohl, 1975) Number of facultative oligotrophic bacteria (CFU/ml) Index FO/H Autopurification ability Total number of Coliform bacteria(CFU/ml) Number of fecal Coliform bacteria(CFU/ml) Water class (Kavka, 1994)
Temerin near the bridge 3660 II 3500 0.96 weak 65 0 unpolluted

Location 2

GPS coordinates: N 45°27’22.51″ E 19°51’14.83″


Physical and chemical parameters at the Jegrička watercourse

ParameterValue
T (°C) 17
O2 (mg 1-1) 0.21
O2(%) 2.3
pH 7.56
CON (µS m-1) 856
TSS (mg 1-1) 13
TOC (mg 1-1) 6.4
NO3- (mg 1-1) <0.5
SUR (mg 1-1) 2
COD (mg 1-1) 17.8
BOD (mg 1-1) 9.3
Transparency (cm) 137
Turbidity (cm) 157

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

GroupsValue
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus 39
Limnodrilus sp. 78
Tubifex tubifex 469
Potamotrix hammoniensis 78
Fam: Naididae
Nais elinguis 39
Nais variabilis
Stylaria lacustris
Ophidonais serpentina
Hirudinea
Helobdella stagnalis
Isopoda
Asellus aquaticus
Ephemeroptera
Fam: Caenidae
Caenis robusta
Odonata
Diptera
Fam: Ceratopogonidae
Bezzia sp.
Fam: Culicidae
Fam: Chironomidae 156
Total number 859

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality Total number of heterotrophi c bacteria(CFU/ml) Water class (kohl, 1975) Number of facultative oligotrophic bacteria (CFU/ml) Index FO/H Autopurification ability Total number of Coliform bacteria(CFU/ml) Number of fecal Coliform bacteria(CFU/ml) Water class (Kavka, 1994)
Temerin near the electrical tower 3650 II 3960 1.09 satisfactory 20 0 unpolluted

Location 3

GPS coordinates: N 45°27’17.66″ E 19°48’40.08″


Physical and chemical parameters at the Jegrička watercourse

ParameterValue
T (°C) 22.2
O2 (mg 1-1) 0.16
O2(%) 1.8
pH 7.43
CON (µS m-1) 571
TSS (mg 1-1) 7.7
TOC (mg 1-1) 3.5
NO3- (mg 1-1) <0.5
SUR (mg 1-1) 1
COD (mg 1-1) 9.8
BOD (mg 1-1) 5
Transparency (cm) 98
Turbidity (cm) to the bottom

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

GroupsValue
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus
Limnodrilus sp. 274
Tubifex tubifex
Potamotrix hammoniensis
Fam: Naididae
Nais elinguis
Nais variabilis
Stylaria lacustris
Ophidonais serpentina
Hirudinea
Helobdella stagnalis
Isopoda
Asellus aquaticus
Ephemeroptera
Fam: Caenidae
Caenis robusta
Odonata
Diptera
Fam: Ceratopogonidae
Bezzia sp. 508
Fam: Culicidae
Fam: Chironomidae 156
Total number 938

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality Total number of heterotrophi c bacteria(CFU/ml) Water class (kohl, 1975) Number of facultative oligotrophic bacteria (CFU/ml) Index FO/H Autopurification ability Total number of Coliform bacteria(CFU/ml) Number of fecal Coliform bacteria(CFU/ml) Water class (Kavka, 1994)
Jegrička - Sirig 1830 II 6750 3.69 satisfactory 820 10 mildly polluted

Location 4

GPS coordinates: N45°26’59.98″ E19°43’36.03″


Physical and chemical parameters at the Jegrička watercourse

ParameterValue
T (°C) 22.1
O2 (mg 1-1) 2.67
O2(%) 38.6
pH 7.28
CON (µS m-1) 582
TSS (mg 1-1) 13.7
TOC (mg 1-1) 3.5
NO3- (mg 1-1) 0.6
SUR (mg 1-1) 1.1
COD (mg 1-1) 10
BOD (mg 1-1) 5
Transparency (cm) 41
Turbidity (cm) 46

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

GroupsValue
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri 117
Limnodrilus claparedeanus 665
Limnodrilus sp. 547
Tubifex tubifex 274
Potamotrix hammoniensis 78
Fam: Naididae
Nais elinguis
Nais variabilis
Stylaria lacustris
Ophidonais serpentina
Hirudinea
Helobdella stagnalis
Isopoda
Asellus aquaticus
Ephemeroptera
Fam: Caenidae
Caenis robusta
Odonata
Diptera
Fam: Ceratopogonidae
Bezzia sp. 78
Fam: Culicidae
Fam: Chironomidae 235
Total number 1994

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality Total number of heterotrophi c bacteria(CFU/ml) Water class (kohl, 1975) Number of facultative oligotrophic bacteria (CFU/ml) Index FO/H Autopurification ability Total number of Coliform bacteria(CFU/ml) Number of fecal Coliform bacteria(CFU/ml) Water class (Kavka, 1994)
Jegrička - Zmajevo 1500 II 8850 5.9 satisfactory 585 195 Very polluted

Location 4

GPS coordinates: N45°27’2.88″ E19°42’13.61″


Physical and chemical parameters at the Jegrička watercourse

ParameterValue
T (°C) 22.2
O2 (mg 1-1) 1.99
O2(%) 21.8
pH 7.55
CON (µS m-1) 575
TSS (mg 1-1) 16.8
TOC (mg 1-1) 3.7
NO3- (mg 1-1) 0.7
SUR (mg 1-1) 0.9
COD (mg 1-1) 10.8
BOD (mg 1-1) 5.3
Transparency (cm) 36
Turbidity (cm) 44

Qualitative and quantitative composition of aquatic macroinvertebrates at the Jergrička watercourse

GroupsValue
Oligochaetae
Fam: Tubificidae
Limnodrilus hoffmeisteri
Limnodrilus claparedeanus
Limnodrilus sp. 587
Tubifex tubifex 117
Potamotrix hammoniensis 117
Fam: Naididae
Nais elinguis
Nais variabilis 39
Stylaria lacustris
Ophidonais serpentina
Hirudinea
Helobdella stagnalis
Isopoda
Asellus aquaticus
Ephemeroptera
Fam: Caenidae
Caenis robusta 39
Odonata
Diptera
Fam: Ceratopogonidae
Bezzia sp.
Fam: Culicidae
Fam: Chironomidae 508
Total number 1407

Results of microbiological analysis (abundance of individual groups of bacteria and their categorization)

Locality Total number of heterotrophi c bacteria(CFU/ml) Water class (kohl, 1975) Number of facultative oligotrophic bacteria (CFU/ml) Index FO/H Autopurification ability Total number of Coliform bacteria(CFU/ml) Number of fecal Coliform bacteria(CFU/ml) Water class (Kavka, 1994)
Jegrička Zmajevo upstream from spillway 11250 II - III 21900 1.95 satisfactory 1052 225 Highly polluted

Location 6

GPS coordinates: N45°26´57.68´´ E19°43´08.88´´


Type of sample: surface water
Sampling location: Jegrička - downstream of station Zmajevo (between 44 and 45 km)
Coordinates of sampling location: N 45°26´57.68´´ E 19°43´08.88´´
Sampling procedure: SRPS ISO 5667-6:1997, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 11:40 -12:30h

Examined parameter Unit of measure Method designation Measured value Class**
Air temperature oC SRPS H.Z1.106:1970 2211
Water temperature oC SRPS H.Z1.106:1970 14,4
Colour* descriptive visual yellowwish, clear
Smell* descriptive visual no
Visible substances* descriptive visual no
pH SRPS H.Z1.111:1987 8,41 I
Electroconductivity µS/cm SRPS EN 27888:2009 700 I
Dissolved oxygen mgO2 /l SRPS EN 5814:2014 2,50 V
Suspended substances mg/l SM 2540 D <12 I
Total dry residue mg/l SM 2540 B 482 I
HPK mgO2/l SRPS ISO 6060:1994 <32 II/III
BPK5 mg O2/l H1.002 5.4 III
Total nitrogen mgN/l H1.011 3,70 III
Total Kjeldahl nitrogen mgN/l H1.003 2,94
Ammonium ion mgN/l SRPS ISO H.Z1.184:1974 0,800 IV
Nitrates mgN/l SRPS ISO 7890-3:1994 0,724 I
Nitrites mgN/l SRPS EN 26777:2009 0,039 III
Total phosphorus mgP/l SRPS EN ISO 6878:2008 0,089 I
Orthophosphates mgP/l SRPS EN ISO 6878:2008 0,062 I
Sulphides mgS/l SM 4500-S2- E <0,5
Anionicdetergents mg/l SRPS EN 903:2009 <0,12 I/II
Carbon Dioxide index mg/l ISO 9377-2:2000(E) <2,02
Metals        
Iron mg/l EPA 7000b 0,414 II
Manganese µg/l EPA 7010 34.2 I
Nickel µg/l EPA 7010 <2,2
Zinc mg/l EPA 7000b <0,023 I
Cadmium µg/l EPA 7010 <0,15
Chromium, total µg/l EPA 7010 <0,90 I
Copper µg/l EPA 7010 16.5 I
Lead µg/l EPA 7010 <5,9
Mercury µg/l H1.004 <0,5
VOC        
Chloroform µg/l H1.001 <1,60
1.1.1-trichloroethane (1.1.1-TCE) µg/l <0,260
1.2-dichloroethane (1.2-DCE) µg/l <0,245
Benzene µg/l <0,365
Trichlorethylene µg/l <0,605
BDHM µg/l <0,480
Toluene µg/l <1,06
DBHM µg/l <0,480
Tetrachloroethylene µg/l <0,510
Chlorobenzene µg/l <0,620
Ethylbenzene µg/l <0,650
m+p-xylene µg/l <0,780
o-xylene µg/l <1,03
Bromoform µg/l <0,720
1,2-dichlorobenzene µg/l <1,15
1,4-dichlorobenzene µg/l <1,32
VinylChloride µg/l <0,500
Pesticidi  
alpha-HCH ng/l SM 6630 <5,00
beta-HCH ng/l <5,00
gamma-HCH (lindane) ng/l <3,25
delta-HCH ng/l <2,50
Heptachlor ng/l <2,50
Heptachlor Epoxide ng/l <2,50
Aldrin ng/l <2,50
Dieldrin ng/l <6,25
Endrin ng/l <6,25
Endrin Aldehyde ng/l <1,75
Endosulfan Sulfate ng/l <2,50
Endosulfan I ng/l <2,50
Endosulfan II ng/l <2,50
4,4´-DDT ng/l <0,500
4,4´-DDD ng/l <2,00
4,4´-DDE ng/l <4,75
Priority pesticides      
Alachlor ng/l EPA 3510C <20,0
Atrazine ng/l <40,0
Simazine ng/l <20,0
Chlorpyrifos ng/l <20,0
Trifluralin ng/l <7,62
Pentachlorobenzene ng/l <5,45
Hexachlorobenzene ng/l <9,67
PAH      
Naphthalene ng/l SM 6440 <10,0
Acenaphthylene ng/l <9,00
Acenaphthene ng/l <10,3
Fluorene ng/l <6,15
Phenanthrene ng/l <6,90
Anthracene ng/l <4,43
Fluoranthene ng/l 22,0
Pyrene ng/l <4.45
Benzo(a)anthracene ng/l <19,1
Chrysene ng/l <20,5
Benzo(b)fluoranthene + Benzo(k)fluoranthene ng/l <24,7
Benzo(a)pyrene ng/l <30,0
Benzo(g,h,i)perylene ng/l <30,0
Dibenzo(a,h)anthracene + Indeno(1,2,3-cd)pyrene ng/l <30,0

*Parameter/method not within accreditation

**According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Type of sample: sadiment
Sampling location: Jegrička - downstream of station Zmajevo (between 44 and 45 km)
Coordinates of sampling location: N 45°26´57.68´´ E 19°43´08.88´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 11:40 -12:30h

Examined parameter Unit of measure Method designation Measured value Corrected value Classifiation**
humidity % SRPS EN 12880:2007 37,0
burned residue % SRPS EN 12879:2007 6,23
granulometry (particles<2µm) % ISO 11277:2009 24,4
pH   SRPS EN 12176:2005      
Redoks potencijal          
Ukupan azot mgN/kg SRPS ISO 11261:2005 1092
organski + amonijačni azot* mgN/kg destilacija i titracija 850
nitratni + nitritni azot* mgN/kg destilacija i titracija 242
Ukupan fosfor mgP/kg spektrofotometrija 298
Metali          
 Nikl mg/kg EPA 7010 36,8 37,4 2
Cink mg/kg EPA 7000b 57,7 61,0 0
Kadmijum mg/kg EPA 7010 0,090 0,100 0
Hrom, ukupan mg/kg EPA 7010 22,6 22,8 0
Bakar mg/kg EPA 7010 21,02 22,7 0
Olovo mg/kg EPA 7010 15,2 16,1 0
Arsen mg/kg EPA 7010 20,2 21,5 0
Živa mg/kg H1.005 0,119 0,120 0
Pesticidi          
alfa-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gama-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptahlor µg/kg <6,53
Heptahlorepoksid µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrinaldehid µg/kg <10,4
Endosulfansulfat µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Prioritetni pesticidi*          
Alahlor µg/kg H1.009 (GC/MSD) <25,0
Atrazin µg/kg <50,0
Simazin µg/kg <25,0
Hlorpirifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentahlorbenzen µg/kg <0,500
Heksahlorbenzen µg/kg <0,500
Alkilfenoli*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-oktilfenol µg/kg <25,0
PAH µg/kg    87   0
Naftalen µg/kg H1.009 (GC/MSD) <4,46
Acenaftilen µg/kg <6,69
Acenaften µg/kg <3,88
Fluoren µg/kg <10,6
Fenantren µg/kg 18,0
Antracen µg/kg <10,8
Fluoranten µg/kg 14,4
Piren µg/kg 15,9
Benzo(a)antracen µg/kg <11,1
Krizen µg/kg <9,88
Benzo(b)fluoranten+ Benzo(k)fluoranten µg/kg 19,7
Benzo(a)piren µg/kg <11,1
Benzo(g,h,i)perilen µg/kg 19,1
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren µg/kg 15,9
PCB (suma) µg/kg H1.008 (GC/µECD) <9,63  0
Dihlorbifenil (PCB 10) µg/kg <9,63
2,4,4´-trihlorbifenil (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrahlorbifenil (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksahlorbifenil  (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180) µg/kg <2,08
Indeks ugljovodonika* mg/kg   174 279 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 7

GPS coordinates: N45°27´22.72´´ E19°53´11.39´´


Type of sample: surface water
Sampling location: Jegrička - near station Temerin
Coordinates of sampling location: N 45°27´22.72´´ E 19°53´11.39´´
Sampling procedure: SRPS ISO 5667-6:1997, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20.04.2018. 09:40-09:50h

Examined parameter Unit of measure Method designation Measured value Class**
Air temperature oC SRPS H.Z1.106:1970 17.3
Water temperature oC SRPS H.Z1.106:1970 14.1
Colour* descriptive visual yellowwish, clear
Smell* descriptive visual no
Visible substances* descriptive visual no
pH SRPS H.Z1.111:1987 8,10 I
Electroconductivity µS/cm SRPS EN 27888:2009 810 I
Dissolved oxygen mgO2 /l SRPS EN 5814:2014 2,70 V
Suspended substances mg/l SM 2540 D <12 I
Total dry residue mg/l SM 2540 B 475 I
HPK mgO2/l SRPS ISO 6060:1994 <32 II/III
BPK5 mg O2/l H1.002 4.3 III
Total nitrogen mgN/l H1.011 2.18 III
Total Kjeldahl nitrogen mgN/l H1.003 1.76
Ammonium ion mgN/l SRPS ISO H.Z1.184:1974 0,706 IV
Nitrates mgN/l SRPS ISO 7890-3:1994 0,392 I
Nitrites mgN/l SRPS EN 26777:2009 0,029 III
Total phosphorus mgP/l SRPS EN ISO 6878:2008 0,032 I
Orthophosphates mgP/l SRPS EN ISO 6878:2008 0,012 I
Sulphides mgS/l SM 4500-S2- E <0,5
Anionicdetergents mg/l SRPS EN 903:2009 <0,12 I/II
Carbon Dioxide index mg/l ISO 9377-2:2000(E) <2,02
Metals        
Iron mg/l EPA 7000b 0,1 II
Manganese µg/l EPA 7010 38.0 I
Nickel µg/l EPA 7010 <2,2
Zinc mg/l EPA 7000b <0,023 I
Cadmium µg/l EPA 7010 <0,15
Chromium, total µg/l EPA 7010 <0,90 I
Copper µg/l EPA 7010 2.19 I
Lead µg/l EPA 7010 <5,9
Mercury µg/l H1.004 <0,5
VOC        
Chloroform µg/l H1.001 <1,60
1.1.1-trichloroethane (1.1.1-TCE) µg/l <0,260
1.2-dichloroethane (1.2-DCE) µg/l <0,245
Benzene µg/l <0,365
Trichlorethylene µg/l <0,605
BDHM µg/l <0,480
Toluene µg/l <1,06
DBHM µg/l <0,480
Tetrachloroethylene µg/l <0,510
Chlorobenzene µg/l <0,620
Ethylbenzene µg/l <0,650
m+p-xylene µg/l <0,780
o-xylene µg/l <1,03
Bromoform µg/l <0,720
1,2-dichlorobenzene µg/l <1,15
1,4-dichlorobenzene µg/l <1,32
VinylChloride µg/l <0,500
Pesticidi  
alpha-HCH ng/l SM 6630 <5,00
beta-HCH ng/l <5,00
gamma-HCH (lindane) ng/l <3,25
delta-HCH ng/l <2,50
Heptachlor ng/l <2,50
Heptachlor Epoxide ng/l <2,50
Aldrin ng/l <2,50
Dieldrin ng/l <6,25
Endrin ng/l <6,25
Endrin Aldehyde ng/l <1,75
Endosulfan Sulfate ng/l <2,50
Endosulfan I ng/l <2,50
Endosulfan II ng/l <2,50
4,4´-DDT ng/l <0,500
4,4´-DDD ng/l <2,00
4,4´-DDE ng/l <4,75
Priority pesticides      
Alachlor ng/l EPA 3510C <20,0
Atrazine ng/l <40,0
Simazine ng/l <20,0
Chlorpyrifos ng/l <20,0
Trifluralin ng/l <7,62
Pentachlorobenzene ng/l <5,45
Hexachlorobenzene ng/l <9,67
PAH      
Naphthalene ng/l SM 6440 <10,0
Acenaphthylene ng/l <9,00
Acenaphthene ng/l <10,3
Fluorene ng/l <6,15
Phenanthrene ng/l <6,90
Anthracene ng/l <4,43
Fluoranthene ng/l 20,3
Pyrene ng/l 22.3
Benzo(a)anthracene ng/l <19,1
Chrysene ng/l <20,5
Benzo(b)fluoranthene + Benzo(k)fluoranthene ng/l <24,7
Benzo(a)pyrene ng/l 65.0
Benzo(g,h,i)perylene ng/l <30,0
Dibenzo(a,h)anthracene + Indeno(1,2,3-cd)pyrene ng/l <30,0

*Parameter/method not within accreditation

**According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 8

GPS coordinates: N45°26´56.90´´ E19°43´14.25´´


Type of sample: sediment
Sampling location: Jegrička - downstream of station Zmajevo (between 44 and 45 km)
Coordinates of sampling location: N 45°26´56.90´´ E 19°43´14.25´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 11:15 -11:30

Examined parameter Unit of measure Method designation Measured value Corrected value Classifiation**
humidity % SRPS EN 12880:2007 38.8
burned residue % SRPS EN 12879:2007 4.92
granulometry (particles<2µm) % ISO 11277:2009 23.2
pH   SRPS EN 12176:2005      
Redoks potencijal          
Ukupan azot mgN/kg SRPS ISO 11261:2005 1246
organski + amonijačni azot* mgN/kg destilacija i titracija 1008
nitratni + nitritni azot* mgN/kg destilacija i titracija 238
Ukupan fosfor mgP/kg spektrofotometrija 273
Metali          
 Nikl mg/kg EPA 7010 41.5 43.7 2
Cink mg/kg EPA 7000b 58.6 64.6 0
Kadmijum mg/kg EPA 7010 0,080 0,090 0
Hrom, ukupan mg/kg EPA 7010 23.9 24.7 0
Bakar mg/kg EPA 7010 23.00 26.0 0
Olovo mg/kg EPA 7010 14.0 15.2 0
Arsen mg/kg EPA 7010 12.5 13.9 0
Živa mg/kg H1.005 0,076 0,080 0
Pesticidi  
alfa-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gama-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptahlor µg/kg <6,53
Heptahlorepoksid µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrinaldehid µg/kg <10,4
Endosulfansulfat µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Prioritetni pesticidi*          
Alahlor µg/kg H1.009 (GC/MSD) <25,0
Atrazin µg/kg <50,0
Simazin µg/kg <25,0
Hlorpirifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentahlorbenzen µg/kg <0,500
Heksahlorbenzen µg/kg <0,500
Alkilfenoli*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-oktilfenol µg/kg <25,0
PAH µg/kg    20   0
Naftalen µg/kg H1.009 (GC/MSD) <4,46
Acenaftilen µg/kg <6,69
Acenaften µg/kg <3,88
Fluoren µg/kg <10,6
Fenantren µg/kg 20.5
Antracen µg/kg <10,8
Fluoranten µg/kg <9.80
Piren µg/kg 13.6
Benzo(a)antracen µg/kg <11,1
Krizen µg/kg <9,88
Benzo(b)fluoranten+ Benzo(k)fluoranten µg/kg 9.23
Benzo(a)piren µg/kg <11,1
Benzo(g,h,i)perilen µg/kg <11.9
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren µg/kg <10.5
PCB (suma) µg/kg H1.008 (GC/µECD) <9,63  0
Dihlorbifenil (PCB 10) µg/kg <9,63
2,4,4´-trihlorbifenil (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrahlorbifenil (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksahlorbifenil  (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180) µg/kg <2,08
Indeks ugljovodonika* mg/kg   159 323 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 9

GPS coordinates: N45°27´33.46´´ E19°52´39.69´´


Type of sample: sediment
Sampling location: Jegrička – at the bridge
Coordinates of sampling location: N 45°27´33.46´´ E 19°52´39.69´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 10:30 -10:40h

Examined parameter Unit of measure Method designation Measured value Corrected value Classifiation**
humidity % SRPS EN 12880:2007 80.5
burned residue % SRPS EN 12879:2007 18.1
granulometry (particles<2µm) % ISO 11277:2009 17.0
pH   SRPS EN 12176:2005      
Redoks potencijal          
Ukupan azot mgN/kg SRPS ISO 11261:2005 5841
organski + amonijačni azot* mgN/kg destilacija i titracija 4576
nitratni + nitritni azot* mgN/kg destilacija i titracija 1265
Ukupan fosfor mgP/kg spektrofotometrija 271
Metali          
 Nikl mg/kg EPA 7010 49.5 64.3 3
Cink mg/kg EPA 7000b 66.1 72.2 0
Kadmijum mg/kg EPA 7010 0.195 0.170 0
Hrom, ukupan mg/kg EPA 7010 31.4 37.4 0
Bakar mg/kg EPA 7010 21.2 27.1 0
Olovo mg/kg EPA 7010 16.5 16.4 0
Arsen mg/kg EPA 7010 37.6 37.5 1
Živa mg/kg H1.005 0,180 0.190 0
Pesticidi  
alfa-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gama-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptahlor µg/kg <6,53
Heptahlorepoksid µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrinaldehid µg/kg <10,4
Endosulfansulfat µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Prioritetni pesticidi*          
Alahlor µg/kg H1.009 (GC/MSD) <25,0
Atrazin µg/kg <50,0
Simazin µg/kg <25,0
Hlorpirifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentahlorbenzen µg/kg <0,500
Heksahlorbenzen µg/kg <0,500
Alkilfenoli*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-oktilfenol µg/kg <25,0
PAH µg/kg   1124   2
Naftalen µg/kg H1.009 (GC/MSD) <4,46
Acenaftilen µg/kg <6,69
Acenaften µg/kg 4.09
Fluoren µg/kg 15.5
Fenantren µg/kg 147
Antracen µg/kg 20.9
Fluoranten µg/kg 237
Piren µg/kg 194
Benzo(a)antracen µg/kg 102
Krizen µg/kg 68.1
Benzo(b)fluoranten+ Benzo(k)fluoranten µg/kg 182
Benzo(a)piren µg/kg 90.5
Benzo(g,h,i)perilen µg/kg 90.4
Dibenzo(a,h)antracen+ Indeno(1,2,3-cd)piren µg/kg 186
PCB (suma) µg/kg H1.008 (GC/µECD) <9,63  0
Dihlorbifenil (PCB 10) µg/kg <9,63
2,4,4´-trihlorbifenil (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrahlorbifenil (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksahlorbifenil (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksahlorbifenil  (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptaahlorbifenil (PCB 180) µg/kg <2,08
Indeks ugljovodonika* mg/kg   157 88 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 10

GPS coordinates: N45°27´30.53´´ E19°52´47.40´´


Type of sample: sediment
Sampling location: Jegrička – upstream from the triangle
Coordinates of sampling location: N 45°27´30.53´´ E 19°52´47.40´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018. 10:15 -10:20h

Examined parameter Unit of measure Method designation Measured value Corrected value Classification**
humidity % SRPS EN 12880:2007 82,8
burned residue % SRPS EN 12879:2007 18,9
granulometry (particles<2µm) % ISO 11277:2009 18,2
pH   SRPS EN 12176:2005      
Redoxpotential          
Total nitrogen mgN/kg SRPS ISO 11261:2005 6703
organic + ammoniacalnitrogen* mgN/kg distillation and titration 4804
nitrate + nitritenitrogen* mgN/kg distillation and titration 1899
Total phosphorus mgP/kg spectrophotometry 277
Metals          
Nickel mg/kg EPA 7010 31,6 39,2 2
Zinc mg/kg EPA 7000b 62,4 65,7 0
Cadmium mg/kg EPA 7010 <0,015 0
Total Chromium mg/kg EPA 7010 27,6 32,0 0
Copper mg/kg EPA 7010 27,0 26,1 0
Lead mg/kg EPA 7010 17,7 17,3 0
Arsenic mg/kg EPA 7010 39,5 38,3 1
Mercury mg/kg H1.005 0,131 0,130 0
Pesticides          
alpha-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gamma-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptachlor µg/kg <6,53
Heptachlor Epoxide µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrin Aldehyde µg/kg <10,4
Endosulfan Sulfate µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Priority pesticides*          
Alachlor µg/kg H1.009 (GC/MSD) <25,0
Atrazine µg/kg <50,0
Simazine µg/kg <25,0
Chlorpyrifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentachlorobenzene µg/kg <0,500
Hexachlorobenzene µg/kg <0,500
Alkylphenols*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-octylphenol µg/kg <25,0
PAH µg/kg    871   0
Naphthalene µg/kg H1.009 (GC/MSD) <4,46
Acenaphthylene µg/kg 9,88
Acenaphthene µg/kg 5,60
Fluorene µg/kg 14,8
Phenanthrene µg/kg 114
Anthracene µg/kg 17,5
Fluoranthene µg/kg 208
Pyrene µg/kg 171
Benz(a)anthracene µg/kg 68,2
Chrysene µg/kg 68,4
Benzo(b)fluoranthene + Benzo(k)fluoranthene µg/kg 168
Benz(a)pyrene µg/kg 73,5
Benzo(g,h,i)perylene µg/kg 49,3
Dibenzo(a,h)anthracene Indeno(1,2,3-cd)pyrene µg/kg 104
PCB (sum) µg/kg H1.008 (GC/µECD) <9,63  0
Dichlor Biphenyl (PCB 10) µg/kg <9,63
2,4,4´-trichloro biphenyl (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrachloro biphenyl (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksachlorbiphenyl (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksachlorbiphenyl (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptachlor biphenyl (PCB 180) µg/kg <2,08
Hydrocarbon Index* mg/kg   209 110 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 11

GPS coordinates: N45°28´02.59´´ E19°54´52.83´´


Type of sample: sediment
Sampling location: Jegrička – 50 m upstream of the Temerin station
Coordinates of sampling location: N 45°28´02.59´´ E 19°54´52.83´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 09:10-09:20h

Examined parameter Unit of measure Method designation Measured value Corrected value Classification**
humidity % SRPS EN 12880:2007 83.4
burned residue % SRPS EN 12879:2007 16.5
granulometry (particles<2µm) % ISO 11277:2009 13.0
pH   SRPS EN 12176:2005      
Redoxpotential          
Total nitrogen mgN/kg SRPS ISO 11261:2005 6962
organic + ammoniacalnitrogen* mgN/kg distillation and titration 4909
nitrate + nitritenitrogen* mgN/kg distillation and titration 2053
Total phosphorus mgP/kg spectrophotometry 303
Metals          
Nickel mg/kg EPA 7010 25.9 39.5 2
Zinc mg/kg EPA 7000b 61.2 75.4 0
Cadmium mg/kg EPA 7010 <0,015 0
Total Chromium mg/kg EPA 7010 25.8 34,0 0
Copper mg/kg EPA 7010 25.4 28.0 0
Lead mg/kg EPA 7010 19.6 20.9 0
Arsenic mg/kg EPA 7010 39.5 42.8 1
Mercury mg/kg H1.005 0.098 0.110 0
Pesticides  
alpha-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gamma-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptachlor µg/kg <6,53
Heptachlor Epoxide µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrin Aldehyde µg/kg <10,4
Endosulfan Sulfate µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Priority pesticides*          
Alachlor µg/kg H1.009 (GC/MSD) <25,0
Atrazine µg/kg <50,0
Simazine µg/kg <25,0
Chlorpyrifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentachlorobenzene µg/kg <0,500
Hexachlorobenzene µg/kg <0,500
Alkylphenols*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-octylphenol µg/kg <25,0
PAH µg/kg    296   0
Naphthalene µg/kg H1.009 (GC/MSD) <4,46
Acenaphthylene µg/kg <6.69
Acenaphthene µg/kg <3.88
Fluorene µg/kg <10.6
Phenanthrene µg/kg 35.4
Anthracene µg/kg <10.8
Fluoranthene µg/kg 55.6
Pyrene µg/kg 48.8
Benz(a)anthracene µg/kg 24.8
Chrysene µg/kg 24.7
Benzo(b)fluoranthene + Benzo(k)fluoranthene µg/kg 65.0
Benz(a)pyrene µg/kg 22.9
Benzo(g,h,i)perylene µg/kg 23.6
Dibenzo(a,h)anthracene Indeno(1,2,3-cd)pyrene µg/kg 44.1
PCB (sum) µg/kg H1.008 (GC/µECD) <9,63  0
Dichlor Biphenyl (PCB 10) µg/kg <9,63
2,4,4´-trichloro biphenyl (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrachloro biphenyl (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksachlorbiphenyl (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksachlorbiphenyl (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptachlor biphenyl (PCB 180) µg/kg <2,08
Hydrocarbon Index* mg/kg   283 172 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

Location 12

GPS coordinates: N45°28´03.0259´´ E19°54´54.94´´


Type of sample: sediment
Sampling location: Jegrička – upstream of Temerin station
Coordinates of sampling location: N 45°28´03.0259´´ E 19°54´54.94´´
Sampling procedure: SRPS ISO 5667-12:2005, SRPS EN ISO 5667-1:2008
Date and time of sampling: 20th April, 2018 09:00 -09:10

Examined parameter Unit of measure Method designation Measured value Corrected value Classification**
humidity % SRPS EN 12880:2007 82.8
burned residue % SRPS EN 12879:2007 17.6
granulometry (particles<2µm) % ISO 11277:2009 21.3
pH   SRPS EN 12176:2005      
Redoxpotential          
Total nitrogen mgN/kg SRPS ISO 11261:2005 5735
organic + ammoniacalnitrogen* mgN/kg distillation and titration 4714
nitrate + nitritenitrogen* mgN/kg distillation and titration 1021
Total phosphorus mgP/kg spectrophotometry 292
Metals          
Nickel mg/kg EPA 7010 31.8 35.6 2
Zinc mg/kg EPA 7000b 61.8 61.7 0
Cadmium mg/kg EPA 7010 0.073 0.060 0
Total Chromium mg/kg EPA 7010 26.4 28.5 0
Copper mg/kg EPA 7010 25.6 24.0 0
Lead mg/kg EPA 7010 15.8 15.1 0
Arsenic mg/kg EPA 7010 39.4 37.4 1
Mercury mg/kg H1.005 0.073 0.070 0
Pesticides  
alpha-HCH µg/kg H1.008 (GC/µECD) <10,1
beta-HCH µg/kg <10,5
gamma-HCH (lindan) µg/kg <7,68
delta-HCH µg/kg <6,53
Heptachlor µg/kg <6,53
Heptachlor Epoxide µg/kg <9,22
Aldrin µg/kg <8,39
Dieldrin µg/kg <7,92
Endrin µg/kg <7,24
Endrin Aldehyde µg/kg <10,4
Endosulfan Sulfate µg/kg <9,88
Endosulfan I µg/kg <5,26
Endosulfan II µg/kg <9,10
4,4´-DDT µg/kg <0,500
4,4´-DDD µg/kg <3,77
4,4´-DDE µg/kg <9,58
Priority pesticides*          
Alachlor µg/kg H1.009 (GC/MSD) <25,0
Atrazine µg/kg <50,0
Simazine µg/kg <25,0
Chlorpyrifos µg/kg <25,0
Trifluralin µg/kg <25,0
Pentachlorobenzene µg/kg <0,500
Hexachlorobenzene µg/kg <0,500
Alkylphenols*          
4-nonilfenol µg/kg H1.009 (GC/MSD) <25,0
4-octylphenol µg/kg <25,0
PAH µg/kg    560   0
Naphthalene µg/kg H1.009 (GC/MSD) <4,46
Acenaphthylene µg/kg <6.69
Acenaphthene µg/kg <3.88
Fluorene µg/kg 11.4
Phenanthrene µg/kg 48.8
Anthracene µg/kg 11.4
Fluoranthene µg/kg 113
Pyrene µg/kg 101
Benz(a)anthracene µg/kg 49.1
Chrysene µg/kg 49.3
Benzo(b)fluoranthene + Benzo(k)fluoranthene µg/kg 132
Benz(a)pyrene µg/kg 58.6
Benzo(g,h,i)perylene µg/kg 37.3
Dibenzo(a,h)anthracene Indeno(1,2,3-cd)pyrene µg/kg 72.3
PCB (sum) µg/kg H1.008 (GC/µECD) <9,63  0
Dichlor Biphenyl (PCB 10) µg/kg <9,63
2,4,4´-trichloro biphenyl (PCB 28) µg/kg <5,26
2,2´,5,5´- tetrachloro biphenyl (PCB 52) µg/kg <7,74
2,2′,3,4,4′,5′-heksachlorbiphenyl (PCB 138) µg/kg <2,81
2,2′,4,4′,5,5′-heksachlorbiphenyl (PCB 153) µg/kg <7,30
2,2′,3,4,4′,5,5′-heptachlor biphenyl (PCB 180) µg/kg <2,08
Hydrocarbon Index* mg/kg   207 118 1

*Parameter/method not within accreditation

** *According to Regulation on emission limit values of polluting substances in surface and groundwaters and sediments and deadlines for their achievement (Official Gazette of the RS 50/2012)

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